HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 44545068, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | N-Hydroxynicotinimidamide | HCID 308113 | — |
| Reactant | 1H-Indazole-5-carboxylic acid | HCID 4248454 | — |
| Product | HCID 44545068 | HCID 44545068 | — |
Reaction Steps
The title compound was prepared according to Method C using 1H-indazole-5-carboxylic acid (ABCR) and N′-hydroxynicotinimidamide (Tyger). 1H NMR (300 MHz, DMSO-d6) δ 7.7 (dd, J=7.9, 4.8 Hz, 1 H), 7.8 (d, J=8.7 Hz, 1 H), 8.2 (dd, J=8.7, 1.6 Hz, 1 H), 8.4 (s, 1 H) 8.5 (dt, J=7.9, 1.8 Hz, 1 H), 8.7 (s, 1 H) 8.8 (dd, J=4.8, 1.6 Hz, 1 H), 9.3 (d, J=2.0 Hz, 1 H), 13.6 (s, 1 H) ppm; MS (DCI/NH3) m/z 264 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486979B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-a4453ad0a0494dd4b5f45a17fd78aca6 |
| Source note | uspto-grants-2013_07 |