HCID 86659591, compound → HCID 89687755, compound

Participants

Reaction Steps

Palladium on carbon (7.8 mg; 10% Pd/C) was added to a solution of the product of step 1 (35 mg, 0.073 mmol) in methanol (2 mL), and the resulting mixture was stirred under hydrogen (balloon) overnight. LC-MS analysis showed the reaction was complete. The reaction mixture was filtered through a microfilter and the filtrate was concentrated under vacuum which was azeotroped from toluene to afford the title compound as a white solid.

Provenance & Evidence