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5-Chloro-3-methyl-1,2,4-thiadiazole → [1-(2,4-Dichloro-phenyl)-5-methyl-1H-[1,2,4]triazol-3-yl]-[1-(3-methyl-[1,2,4]thiadiazol-5-yl)-piperidin-4-yl]-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Chloro-3-methyl-1,2,4-thiadiazole | HCID 12919159 | — |
| 反応物 | HCID 67342750 | HCID 67342750 | — |
| 生成物 | [1-(2,4-Dichloro-phenyl)-5-methyl-1H-[1,2,4]triazol-3-yl]-[1-(3-methyl-[1,2,4]thiadiazol-5-yl)-piperidin-4-yl]-amine | HCID 67343081 | — |
反応手順
Prepared in analogy to example 1 step b) starting from [1-(2,4-dichloro-phenyl)-5-methyl-1H-[1,2,4]triazol-3-yl]-piperidin-4-yl-amine hydrochloride and 5-chloro-3-methyl-[1,2,4]thiadiazole (example 1 step a)). The title compound was obtained as slightly yellow solid (yield=10%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08486967B2 |
| 出典データセット | uspto-grants-2013_07 |
| ORD ID | ord-91f5044c1bd346708288e96c0550ca3d |
| 出典メモ | uspto-grants-2013_07 |