Ethyl chloroformate → HCID 67342920, compound

Participants

Reaction Steps

Prepared in analogy to example 164b, starting from 6-methyl-N-(1-(6-methylpyrimidin-4-yl)piperidin-4-yl)-8-(1,2,3,6-tetrahydropyridin-4-yl)-[1,2,4]triazolo[1,5-a]pyridin-2-amine and ethyl chloroformate. The title compound was obtained as a light yellow solid (yield: 36%) after column chromatography on silica gel using a gradient from methylene chloride to a mixture of methylene chloride/methanol 19:1 (v/v) as eluent.

Provenance & Evidence