HCID 59201311, compound → HCID 59201539, compound

Participants

Reaction Steps

A solution of tert-butyl (2S,3R)-3-azido-1-cyclohexylpentan-2-ylcarbamate (64 mg, 0.21 mmol) and 10% Pd/C in methanol (20 mL) was hydrogenated at 40 psi for 1 h. The catalyst was filtered off, and the filtrate concentrated to give tert-butyl (2S,3R)-3-amino-1-cyclohexylpentan-2-ylcarbamate (55 mg, 93%). MS ESI +ve m/z 285 (M+H).

Provenance & Evidence