HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentane → HCID 86643015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentane | HCID 8003 | — |
| Reactant | Propane, 2-fluoro-2-methyl- | HCID 9626 | — |
| Product | HCID 86643015 | HCID 86643015 | — |
Reaction Steps
Approximately 220 mL of cold n-pentane kept at 0° C. was poured in a glass graduated cylinder. To the n-pentane was added approximately 1.7 mL of tert-butyl fluoride which was also kept at 0° C. The solution was mixed thoroughly and analyzed by CAP-GC using the CGSB (Canadian General Standards Board, 3.0 14.3-99) method for gasoline. The concentration of tert-butyl fluoride was 0.615 vol %. The solution was kept in the refrigerator at 0° C. Lower concentrations of the tert-butyl fluoride-n-pentane stock solution was obtained by diluting with pentane. To obtain 0.45 vol % of tert-butyl fluoride, 60.5 mL of n-pentane was added to 159.5 mL of the stock solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08487155B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-573b1731380d4fca9f535a8f1c01009b |
| Source note | uspto-grants-2013_07 |