HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178517952, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 5-Aminobenzimidazole | HCID 13623 | — |
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | Trimethylsilyl cyanide | HCID 82115 | — |
| Reactant | 2,3,5-Trifluorobenzaldehyde | HCID 2776950 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Product | HCID 178517952 | HCID 178517952 | — |
Reaction Steps
The compound was synthesized starting from 5-aminobenzimidazole (0.732 g, 5.5 mmol), 2,3,5-trifluorobenzaldehyde (0.57 mL, 5 mmol), TMSCN (0.625 mL, 5 mmol), concentrated aqueous HCl (15 mL), triethyl orthoformate (30 mL, excess), NaBH4 (0.157 g, 4.14 mmol) as described in method 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486940B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-e267de157ed245c98df1f1dc3ed94cdd |
| Source note | uspto-grants-2013_07 |