HuagongsheHuagongshe Chemistry Print Report · For research reference only
Veratraldehyde → HCID 178488768, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Veratraldehyde | HCID 8419 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | Trimethylsilyl cyanide | HCID 82115 | — |
| Reactant | HCID 178507353 | HCID 178507353 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 178488768 | HCID 178488768 | — |
Reaction Steps
The compound was synthesized starting from 1H-benzo[d]imidazol-5-amine (0.400 g, 3 mmol), 3,4-dimethoxybenzaldehyde (0.5 g, 3 mmol), TMSCN (0.375 mL, 3 mmol), Pd/C (10%, 0.02 g), TEA 1.05 mL, 7.5 mmol), di-(imidazol-1-yl)methanone (0.730 g, 4.5 mmol) as described in method 2 to give 1-(1H-benzo[d]imidazol-5-yl)-5-(3,4-dimethoxyphenyl)imidazolidin-2-one
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486940B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-c9cc824081a2418eae0eff4fd78f77fe |
| Source note | uspto-grants-2013_07 |