HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminobenzimidazole → HCID 178458238, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminobenzimidazole | HCID 13623 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | Trimethylsilyl cyanide | HCID 82115 | — |
| Reactant | 3-Fluoro-4-propoxybenzaldehyde | HCID 57431926 | — |
| Product | HCID 178458238 | HCID 178458238 | — |
Reaction Steps
The compound was further synthesized starting from 5-aminobenzimidazole (0.806 g, 6.1 mmol), 3-fluoro-4-propoxybenzaldehyde (1.0 g, 5.5 mmol), TMSCN (0.69 mL, 5.5 mmol), PdC (10%, 0.02 g), TEA 1.44 mL, 10.3 mmol), di-(imidazol-1-yl)methanone (0.92 g, 5.6 mmol) as described in method 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486940B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-b58736d4e7e146c382682e22e6c89526 |
| Source note | uspto-grants-2013_07 |