HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-5-nitrobenzotrifluoride → HCID 59536608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-5-nitrobenzotrifluoride | HCID 94954 | — |
| Reactant | 3-({[tert-Butyl(diphenyl)silyl]oxy}methyl)pyridin-2(1H)-one | HCID 59410156 | — |
| Product | HCID 59536608 | HCID 59536608 | — |
Reaction Steps
Analogously to Example 4A, 1.50 g (4.13 mmol) of the compound from Example 3A are reacted with 949 mg (4.54 mmol) of 1-fluoro-4-nitro-2-(trifluoromethyl)benzene. The product is purified by chromatography on silica gel (mobile phase pentane/ethyl acetate=5:1), giving 1.00 g (44% of theory) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08487111B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-c77fc65469654613b8a9fd305172dbcf |
| Source note | uspto-grants-2013_07 |