HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethylamine → HCID 44481903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | 2-(bromomethyl)-7-(methylsulfonyl)-4H-1,3-benzodioxine | HCID 66886440 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 44481903 | HCID 44481903 | — |
Reaction Steps
Preparation according to Example 22 using 2-(bromomethyl)-7-(methylsulfonyl)-4H-1,3-benzodioxine (30 mg, 0.10 mmol), 2-methyoxyethanamine (0.50 ml, 5.8 mmol) and EtOH (1.0 ml). MS m/z (rel. intensity, 70 eV) 301 (M+, 1), 123 (13), 88 (bp), 72 (25), 56 (13).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492372B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-e25f10637ee3413ebb854646b82bf53c |
| Source note | uspto-grants-2013_07 |