HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 44481904, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 2-(bromomethyl)-7-(methylsulfonyl)-4H-1,3-benzodioxine | HCID 66886440 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 44481904 | HCID 44481904 | — |
Reaction Steps
Preparation according to Example 22 using 2-(bromomethyl)-7-(methylsulfonyl)-4H-1,3-benzodioxine (30 mg, 0.10 mmol), N-ethylethanamine (0.50 ml, 4.8 mmol) and EtOH (1.0 ml). MS m/z (rel. intensity, 70 eV) 299 (M+, 1), 87 (6), 86 (bp), 77 (4), 58 (6).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492372B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-585836c79ce74f81a7a13740e5ac5b44 |
| Source note | uspto-grants-2013_07 |