HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 44482179, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 2-(bromomethyl)-5-fluoro-7-(methylsulfonyl)-4H-1,3-benzodioxine | HCID 66887621 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 44482179 | HCID 44482179 | — |
Reaction Steps
Preparation according to Example 34 using 2-(bromomethyl)-5-fluoro-7-(methylsulfonyl)-4H-1,3-benzodioxine (7 mg, 0.021 mmol), pyrrolidine (0.5 ml) and EtOH (1.0 ml). MS m/z (rel. intensity, 70 eV) 315 (M+, 0.5), 95 (4), 85 (6), 84 (bp), 75 (4), 55 (7).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492372B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-6236eb4491fd409eb5412b50c50df508 |
| Source note | uspto-grants-2013_07 |