HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → HCID 44482180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | 2-(bromomethyl)-5-fluoro-7-(methylsulfonyl)-4H-1,3-benzodioxine | HCID 66887621 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 44482180 | HCID 44482180 | — |
Reaction Steps
Preparation according to Example 34 using 2-(bromomethyl)-5-fluoro-7-(methylsulfonyl)-4H-1,3-benzodioxine (7 mg, 0.021 mmol), prop-2-en-1-amine (0.5 ml) and EtOH (3 ml). MS m/z (rel. intensity, 70 eV) 301 (M+, 0.4), 141 (9), 95 (8), 75 (8), 71 (6), 70 (bp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492372B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-9d909245ee2f428cba4a3c0843f81aaa |
| Source note | uspto-grants-2013_07 |