HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → N-{(1R,3S)-3-[(benzyloxy)methyl]cyclopentyl}-6-chloro-N-methylpyridine-3-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 46701889 | HCID 46701889 | — |
| Reactant | HCID 86659753 | HCID 86659753 | — |
| Product | N-{(1R,3S)-3-[(benzyloxy)methyl]cyclopentyl}-6-chloro-N-methylpyridine-3-sulfonamide | HCID 86659752 | 86% |
Reaction Steps
According to process 23.2, starting with 0.66 g of 4 N-{(1R,3S)-3-[(benzyloxy)methyl]cyclopentyl}-6-chloropyridine-3-sulfonamide and 0.22 mL of methyl iodide, 0.58 g of N-{(1R,3S)-3-[(benzyloxy)methyl]cyclopentyl}-6-chloro-N-methylpyridine-3-sulfonamide is obtained in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08541455B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-48a7993569234b09b01c2e162858ac2c |
| Source note | uspto-grants-2013_09 |