HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methylthio)phenylboronic acid → Methyl 3-[4-(methylthio)phenyl]-1-benzofuran-5-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methylthio)phenylboronic acid | HCID 2733959 | — |
| Reactant | Methyl 3-bromo-1-benzofuran-5-carboxylate | HCID 22481688 | — |
| Product | Methyl 3-[4-(methylthio)phenyl]-1-benzofuran-5-carboxylate | HCID 44482027 | 92% |
Reaction Steps
In the same manner as in Reference Example 19 and using methyl 3-bromo-1-benzofuran-5-carboxylate instead of methyl 3-iodoimidazo[1,2-a]pyridine-6-carboxylate and 4-(methylthio)phenylboronic acid instead of (4-methoxyphenyl)boronic acid, the title compound (yield 92%) was obtained as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492378B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-a4d66102a7ea47b59eab07558e873a3c |
| Source note | uspto-grants-2013_07 |