Water → HCID 68664688, compound

Participants

Reaction Steps

A suspension of 2-fluoro-4-[5-(5-methyl-1,3,4-oxadiazol-2-yl)-1-benzofuran-3-yl]benzaldehyde (0.693 g, 2.15 mmol) and oxone (registered trade mark) (1.99 g, 3.23 mmol) in N,N-dimethylformamide (25 mL) was stirred overnight at room temperature. The reaction mixture was poured into water, and the precipitate was collected by filtration, dried and recrystallized from tetrahydrofuran to give the title compound (555 mg, yield 76%) as colorless crystals.

Provenance & Evidence