HCID 68663743, compound → HCID 68663145, compound

HRID 452727Notes

Reaction equation

HRID 452727 reaction equation
[CH3:1][C:2]1[O:6][C:5]([C:7]2[CH:8]=[CH:9][C:10]3[O:14][CH:13]=[C:12]([C:15]([O:17]CC)=[O:16])[C:11]=3[CH:20]=2)=[N:4][N:3]=1>C(O)C>[CH3:1][C:2]1[O:6][C:5]([C:7]2[CH:8]=[CH:9][C:10]3[O:14][CH:13]=[C:12]([C:15]([OH:17])=[O:16])[C:11]=3[CH:20]=2)=[N:4][N:3]=1

Participants

3

Reactant 1

HCID 68663743HCID 68663743, compound

Product 1

HCID 68663145HCID 68663145, compoundYield 32%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In the same manner as in Example 134 and using ethyl 5-(5-methyl-1,3,4-oxadiazol-2-yl)-1-benzofuran-3-carboxylate instead of methyl 4-[5-(5-methyl-1,3,4-oxadiazol-2-yl)-1-benzofuran-3-yl]benzoate and ethanol instead of methanol, the title compound (yield 32%) was obtained as pale-yellow crystals.

Sources & evidence

ORD record
ord-314f572e7eb34dcd8319762c67c0ffde
Source dataset
uspto-grants-2013_07
Patent number
US08492378B2

Reaction notes

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