化工社化工社 化学情報印刷レポート · 研究参考用
4-Methyloxybenzyl chloride → 2-[(4-Methoxybenzyl)thio]-5-[3-(4-methoxyphenyl)-1-benzofuran-5-yl]-1,3,4-oxadiazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| 反応物 | HCID 178488802 | HCID 178488802 | — |
| 生成物 | 2-[(4-Methoxybenzyl)thio]-5-[3-(4-methoxyphenyl)-1-benzofuran-5-yl]-1,3,4-oxadiazole | HCID 68663924 | 80% |
反応手順
In the same manner as in Example 1 and using 5-[3-(4-methoxyphenyl)-1-benzofuran-5-yl]-1,3,4-oxadiazole-2-thiol instead of 5-(benzothiazol-6-yl)-1,3,4-oxadiazole-2-thiol and 4-methoxybenzyl chloride instead of 3-(trifluoromethyl)benzyl chloride, the title compound (yield 80%) was obtained as colorless crystals.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08492378B2 |
| 出典データセット | uspto-grants-2013_07 |
| ORD ID | ord-7057a2e0fc344e51ac0211f211d63a30 |
| 出典メモ | uspto-grants-2013_07 |