HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 45123408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 1-Methylcyclopropanecarboxylic acid | HCID 81326 | — |
| Reactant | Thiosemicarbazide | HCID 2723789 | — |
| Product | HCID 45123408 | HCID 45123408 | — |
Reaction Steps
Commercially available, 1-methyl-cyclopropane-1-carboxylic acid (Aldrich), thiosemicarbazide (Aldrich) and phosphorus oxychloride (Aldrich) were processed as described for Example 1A to obtain the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 0.84-0.93 (m, 2H), 0.93-1.03 (m, 2H), 1.41 (s, 3H), 6.94 (s, 2H); MS (ESI+) m/z 156 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492371B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-c02db6c0524d4cfe818654f2b0a170be |
| Source note | uspto-grants-2013_07 |