HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 71650980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | Thiosemicarbazide | HCID 2723789 | — |
| Reactant | 2,2-Dimethylbut-3-ynoic acid | HCID 13905647 | — |
| Product | HCID 71650980 | HCID 71650980 | — |
Reaction Steps
Commercially available, 2,2-dimethylbut-3-ynoic acid (Betapharma), thiosemicarbazide (Aldrich) and phosphorus oxychloride (Aldrich) were processed as described for Example 1A to obtain the title compound. MS (ESI+) m/z 168 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492371B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-47ad2375dd0246fcb18f820f0ef3d22e |
| Source note | uspto-grants-2013_07 |