HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Azathymine → 2-(4-Chloro-butyl)-6-methyl-2H-[1,2,4]triazine-3,5-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Azathymine | HCID 70269 | — |
| Reactant | 1-Bromo-4-chlorobutane | HCID 81364 | — |
| Reactant | 6-Azathymine, TMS | HCID 529003 | — |
| Reactant | 2-(4-Chloro-butyl)-2H-[1,2,4]triazine-3,5-dione | HCID 15817175 | — |
| Product | 2-(4-Chloro-butyl)-6-methyl-2H-[1,2,4]triazine-3,5-dione | HCID 59614492 | — |
Reaction Steps
2-(4-Chloro-butyl)-6-methyl-2H-[1,2,4]triazine-3,5-dione were synthesized as described for the synthesis of 2-(4-Chloro-butyl)-2H-[1,2,4]triazine-3,5-dione starting from 6-methyl-2H-[1,2,4]triazine-3,5-dione which was converted into 6-methyl-3,5-bis-trimethylsilanyloxy-[1,2,4]triazine by the method described in working example 1 and thereafter reacted with 1-bromo-4-chloro-butane according to working example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492540B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-50bfb271c00f4946b066c9e3d594c39b |
| Source note | uspto-grants-2013_07 |