HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66727278, compound → HCID 25174350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66727278 | HCID 66727278 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 25174350 | HCID 25174350 | 75.3% |
Reaction Steps
(R)-2,3-Dihydrobenzo[1,4]dioxin-2-yl-[(S*)-3-(2-fluorophenyl)piperidin-1-yl]methanone (25 mg, 0.073 mmol) was treated with BH3 THF according to the above general procedure. Flash chromatography gave 18 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492549B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-671f34a6b25d4067ad2686722ffafd48 |
| Source note | uspto-grants-2013_07 |