HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 25175496, compound → HCID 25175497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 25175496 | HCID 25175496 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 25175497 | HCID 25175497 | — |
Reaction Steps
The above described 2-(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)-1,2,3,4,5,6,7,8-octahydroisoquinoline (195 mg, 0.68 mmol) was hydrogenated in MeOH (20 ml) under normal pressure (12 h, 50° C.) to give the crude title compound, which was purified by flash chromatography (heptane/EtOAc).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492549B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-72285994ed564963b584917dab9b1d6c |
| Source note | uspto-grants-2013_07 |