Sodium Hydroxide → HCID 58508800, compound

HRID 454567Notes

Reaction equation

HRID 454567 reaction equation
[OH-].[Na+:2].[O:3]1[CH:7]=[CH:6][CH:5]=[C:4]1[C:8]1[CH:16]=[CH:15][C:11]([C:12]([OH:14])=[O:13])=[C:10]([NH:17][C:18](=[O:28])[C:19]2[CH:24]=[C:23]([O:25][CH3:26])[CH:22]=[CH:21][C:20]=2[OH:27])[CH:9]=1>C(O)C>[O:3]1[CH:7]=[CH:6][CH:5]=[C:4]1[C:8]1[CH:16]=[CH:15][C:11]([C:12]([O-:14])=[O:13])=[C:10]([NH:17][C:18](=[O:28])[C:19]2[CH:24]=[C:23]([O:25][CH3:26])[CH:22]=[CH:21][C:20]=2[OH:27])[CH:9]=1.[Na+:2]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 58508801HCID 58508801, compound

Product 1

HCID 58508800HCID 58508800, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Ethanol (2.5 mL) and a 1 mol/L aqueous solution of sodium hydroxide (0.17 mL) were added to the obtained 4-(furan-2-yl)-2-(2-hydroxy-5-methoxybenzamido)benzoic acid (0.062 g), followed by stirring at room temperature for 35 minutes. The solid substance was collected by filtration to obtain 0.046 g of sodium 4-(furan-2-yl)-2-(2-hydroxy-5-methoxybenzamido)benzoate as a white solid.

Workup

  1. filtrationThe solid substance was collected by filtration

Sources & evidence

ORD record
ord-1fec6bf444a6422c87dcda15558fc2f2
Source dataset
uspto-grants-2013_07
Patent number
US08492582B2

Reaction notes

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