Sodium Hydroxide → HCID 58508944, compound

HRID 454569Notes

Reaction equation

HRID 454569 reaction equation
[OH-].[Na+:2].[O:3]1[CH:7]=[CH:6][C:5]([C:8]2[CH:16]=[CH:15][C:11]([C:12]([OH:14])=[O:13])=[C:10]([NH:17][C:18](=[O:32])[C:19]3[CH:24]=[C:23]([C:25]4[CH:26]=[N:27][CH:28]=[CH:29][CH:30]=4)[CH:22]=[CH:21][C:20]=3[OH:31])[CH:9]=2)=[CH:4]1>C(O)C>[O:3]1[CH:7]=[CH:6][C:5]([C:8]2[CH:16]=[CH:15][C:11]([C:12]([O-:14])=[O:13])=[C:10]([NH:17][C:18](=[O:32])[C:19]3[CH:24]=[C:23]([C:25]4[CH:26]=[N:27][CH:28]=[CH:29][CH:30]=4)[CH:22]=[CH:21][C:20]=3[OH:31])[CH:9]=2)=[CH:4]1.[Na+:2]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 58508945HCID 58508945, compound

Product 1

HCID 58508944HCID 58508944, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Ethanol (1.5 mL) and a 1 mol/L aqueous solution of sodium hydroxide (0.19 mL) were added to the obtained 4-(furan-3-yl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoic acid (0.081 g), followed by stirring at room temperature for 1 hour. The solid substance was collected by filtration to obtain 0.048 g of sodium 4-(furan-3-yl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoate as a white solid.

Workup

  1. filtrationThe solid substance was collected by filtration

Sources & evidence

ORD record
ord-315f3864945047bcad3500fb780839f3
Source dataset
uspto-grants-2013_07
Patent number
US08492582B2

Reaction notes

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