HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 58508458, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 58508444 | HCID 58508444 | — |
| Product | HCID 58508458 | HCID 58508458 | 89.3% |
Reaction Steps
Trifluoroacetic acid (5 mL) was added to the obtained tert-butyl 2-(5-phenylpyridine-3-carboxamido)-4-(1H-pyrazol-1-yl)benzoate (68 mg), followed by stirring at room temperature for 4 hours. The solvent was evaporated under reduced pressure, and methanol was added to the obtained residue. The solid substance was collected by filtration to obtain 53 mg of 2-(5-phenylpyridine-3-carboxamido)-4-(1H-pyrazol-1-yl)benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492582B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-adf6e0247a8341d2a6c66223884b72f3 |
| Source note | uspto-grants-2013_07 |