Sodium Hydroxide → HCID 58508707, compound

HRID 454738Notes

Reaction equation

HRID 454738 reaction equation
[OH-].[Na+:2].[C:3]1([C:9]2[CH:10]=[C:11]([C:15]([NH:17][C:18]3[CH:26]=[C:25]([C:27]4[CH:32]=[CH:31][CH:30]=[CH:29][N:28]=4)[CH:24]=[CH:23][C:19]=3[C:20]([OH:22])=[O:21])=[O:16])[CH:12]=[N:13][CH:14]=2)[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>C(O)C>[C:3]1([C:9]2[CH:10]=[C:11]([C:15]([NH:17][C:18]3[CH:26]=[C:25]([C:27]4[CH:32]=[CH:31][CH:30]=[CH:29][N:28]=4)[CH:24]=[CH:23][C:19]=3[C:20]([O-:22])=[O:21])=[O:16])[CH:12]=[N:13][CH:14]=2)[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1.[Na+:2]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 58508708HCID 58508708, compound

Product 1

HCID 58508707HCID 58508707, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Ethanol (2.0 mL) and a 2 mol/L aqueous solution of sodium hydroxide (0.094 mL) were sequentially added to the obtained 2-(5-phenylpyridine-3-carboxamido)-4-(pyridin-2-yl)benzoic acid (74 mg), followed by stirring at room temperature for 1 hour and 30 minutes. The solid substance was collected by filtration to obtain 59 mg of sodium 2-(5-phenylpyridine-3-carboxamido)-4-(pyridin-2-yl)benzoate as a white solid.

Workup

  1. filtrationThe solid substance was collected by filtration

Sources & evidence

ORD record
ord-8c8717e761614a5eb60802ca404c8c31
Source dataset
uspto-grants-2013_07
Patent number
US08492582B2

Reaction notes

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