Sodium Hydroxide → HCID 58508773, compound

HRID 454746Notes

Reaction equation

HRID 454746 reaction equation
[OH-].[Na+:2].[O:3]1[CH:7]=[CH:6][CH:5]=[C:4]1[C:8]1[CH:16]=[CH:15][C:11]([C:12]([OH:14])=[O:13])=[C:10]([NH:17][C:18]([C:20]2[CH:21]=[N:22][CH:23]=[C:24]([C:26]3[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=3)[CH:25]=2)=[O:19])[CH:9]=1>C(O)C>[O:3]1[CH:7]=[CH:6][CH:5]=[C:4]1[C:8]1[CH:16]=[CH:15][C:11]([C:12]([O-:14])=[O:13])=[C:10]([NH:17][C:18]([C:20]2[CH:21]=[N:22][CH:23]=[C:24]([C:26]3[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=3)[CH:25]=2)=[O:19])[CH:9]=1.[Na+:2]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 58508774HCID 58508774, compound

Product 1

HCID 58508773HCID 58508773, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Ethanol (4.5 mL) and a 2 mol/L aqueous solution of sodium hydroxide (0.085 mL) were added to the obtained 4-(furan-2-yl)-2-(5-phenylpyridine-3-carboxamido)benzoic acid (69 mg), followed by stirring at room temperature for 1 hour and 20 minutes. The solid substance was collected by filtration to obtain 31 mg of sodium 4-(furan-2-yl)-2-(5-phenylpyridine-3-carboxamido)benzoate as a white solid.

Workup

  1. filtrationThe solid substance was collected by filtration

Sources & evidence

ORD record
ord-e4631e2a3b9c418f892e6c07f4eef7eb
Source dataset
uspto-grants-2013_07
Patent number
US08492582B2

Reaction notes

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