HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,6-Dichloropyridazine → 6-chloro-N,N-dimethylpyridazin-3-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,6-Dichloropyridazine | HCID 67331 | — |
| Edukt | Dimethylamine methanol | HCID 22497844 | — |
| Produkt | 6-chloro-N,N-dimethylpyridazin-3-amine | HCID 252474 | 96,3% |
Reaktionsschritte
3-(N,N-Dimethylamino)-6-chloropyridazine (108f, 510 mg, 96%) was prepared in the same manner as in Example 29 as a white solid using 3,6-dichloropyridazine (107, 500 mg, 3.36 mmol) and a 2.0 M dimethylamine methanol solution (NHMe2 in MeOH, 5 mL, 10 mmol).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08497260B2 |
| Quelldatensatz | uspto-grants-2013_07 |
| ORD ID | ord-3fdef52f4ff9423e9c292be350d38a88 |
| Quellennotiz | uspto-grants-2013_07 |