Hexahydro-1,4-diazepine → HCID 178515205, compound

Participants

Reaction Steps

The title compound was prepared following the procedure described for 6a using perhydro-[1,4]-diazepine instead of piperazine. 1H-NMR (DMSO-d6) δ (ppm): 1.82 (2H, m), 2.65 (2H, m), 2.90 (2H, m), 3.88 (4H, m), 6.89 (1H, d, J=9.07 Hz), 7.05 (1H, t, J=7.41 Hz), 7.35 (2H, dd, J=8.52, 7.41 Hz), 7.74 (1H, d, J=9.07 Hz), 8.25 (2H, m), 8.29 (1H, s). m/z 361.4 (MH+).

Provenance & Evidence