HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperazine → HCID 178492065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperazine | HCID 4837 | — |
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 178492064 | HCID 178492064 | — |
| Reactant | HCID 178515211 | HCID 178515211 | — |
| Product | HCID 178492065 | HCID 178492065 | — |
Reaction Steps
The title compound was prepared following the procedure described for 6a using 5c and 1-methylpiperazine instead of 5a and piperazine respectively. 1H-NMR (DMSO-d6) δ (ppm): 2.22 (3H, s), 2.56 (4H, m), 3.64 (4H, m), 6.98 (2H, d, J=9.07 Hz), 7.15 (1H, d, J=9.34 Hz), 7.78 (6H, d, J=9.34 Hz), 8.10 (2H, d, J=9.07 Hz), 8.45 (1H, s). m/z 391.4 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497262B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-4fc7f9ca23a1483bae464842ce422a59 |
| Source note | uspto-grants-2013_07 |