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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 454983Generated: October 30, 2026

HCID 67073791, compound → HCID 66513497, compound

https://huagongshe.com/reaction/454983

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67073791HCID 67073791—
CatalystPalladiumHCID 23938—
SolventEthylacetate methanolHCID 21584119—
ProductHCID 66513497HCID 66513497100%

Reaction Steps

A mixture of [(R)-1-(4-Benzyloxy-2-methoxy-phenyl)-2-hydroxy-ethyl]-carbamic acid benzyl ester (1.2 g, 2.96 mmol) and Pd/C (120 mg) in MeOH/EtOAc (5:1, 10 mL) was stirred under H2 (1 atm) for overnight. The mixture was filtered and the filtrate was concentrated to give the titled compound (542 mg, 100%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08497271B2
Source datasetuspto-grants-2013_07
ORD IDord-97eddcb5770e4aae98520da6377e8ae5
Source noteuspto-grants-2013_07