Dimethylamine → 2,2-Bis(4-chlorophenyl)-N,N-dimethylacetamide

HRID 45502Notes

Reaction equation

HRID 45502 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]([C:12]2[CH:17]=[CH:16][C:15]([Cl:18])=[CH:14][CH:13]=2)[C:9](O)=[O:10])=[CH:4][CH:3]=1.[CH3:19][NH:20][CH3:21]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]([C:12]2[CH:17]=[CH:16][C:15]([Cl:18])=[CH:14][CH:13]=2)[C:9]([N:20]([CH3:21])[CH3:19])=[O:10])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 674DimethylamineHCID 6730Bis(4-chlorophenyl)acetic acid

Product 1

HCID 5518692,2-Bis(4-chlorophenyl)-N,N-dimethylacetamide

Procedure

Bis-(4-chloro-phenyl)-acetic acid was reacted with dimethylamine following the procedure set out in Example 8D to give the title compound. LC/MS: (PS-A2) Rt 3.40 [M+H]+ 309.95.

Sources & evidence

ORD record
ord-fe6f138521b14120bb9548a255073b25
Source dataset
uspto-grants-2013_09
Patent number
US08541461B2

Reaction notes

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