HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 67028755, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 2-(6-Methyl-2-p-tolyl-imidazo[1,2-a]pyridin-3-ylmethyl)-2H-[1,2,4]triazole-3-carboxylic acid methylamide | HCID 67027485 | — |
| Reactant | HCID 67028756 | HCID 67028756 | — |
| Product | HCID 67028755 | HCID 67028755 | — |
Reaction Steps
The title compound was prepared according to the procedure described for compound 68 from 3 methyl 1-((2-(4-chlorophenyl)imidazo[1,2-a]pyridin-3-yl)methyl)-3-methyl-1H-pyrazole-5-carboxylate and methylamine. M/e+ 380 for C20H19ClN5O (M+H)+; 1H-NMR (400 MHz, CDCl3) δ 8.29 (d, J=6.6 Hz, 1H), 7.85 (d, J=8.4 Hz, 2H), 7.64 (d, J=8.8 Hz, 1H), 7.42 (d, J=8.4 Hz, 2H), 7.23 (m, 1H), 6.82 (t, J=6.9 Hz, 1H), 6.66 (s, 1H), 6.05 (s, 2H), 3.84 (s, 3H), 2.19 (s, 3H) 1.57 (s, 1H), ppm;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497278B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-bca98fa7bdcc407fa018ac12b9e97397 |
| Source note | uspto-grants-2013_07 |