N,N-Dimethylethylenediamine → HCID 67028936, compound

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Reaction Steps

The title compound was prepared according to the experimental for compound 132 from 4-chloro-1-((2-(4-chlorophenyl)imidazo[1,2-a]pyridin-3-yl)methyl)pyrimidin-2(1H)-one and N1,N1-dimethylethane-1,2-diamine. M/e+ 423 for C22H24ClN6O (M+H)+; 1H-NMR (400 MHz, CDCl3) δ 8.42 (d, J=6.9 Hz, 1H), 7.68 (dd, J=8.4, 2.2 Hz, 2H), 7.64 (dd, J=9.1, 1.1 Hz, 1H), 7.47 (dd, J=8.4, 2.2 Hz, 2H), 7.28 (d, J=7.7 Hz, 1H), 6.86 (t, J=6.6 Hz, 1H), 6.65 (dd, J=7.3, 2.2 Hz, 1H), 6.49 (bs, 1H), 5.54 (d, J=1.8 Hz, 2H), 5.46 (dd, J=7.3, 1.8 Hz, 1H), 3.59 (m, 2H), 2.61 (m, 2H), 2.16 (s, 6H) ppm.

Provenance & Evidence