HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetamidine monohydrochloride → HCID 178434008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetamidine monohydrochloride | HCID 67170 | — |
| Reactant | 2-(2-(4-Chlorophenyl)imidazo[1,2-a]pyridin-3-yl)acetohydrazide | HCID 67029159 | — |
| Reactant | HCID 178477970 | HCID 178477970 | — |
| Product | HCID 178434008 | HCID 178434008 | — |
Reaction Steps
The title compound was prepared according to the experimental described for compound 230 from 2-(2-(4-chlorophenyl)imidazo[1,2-a]pyridin-3-yl)acetohydrazide and acetimidamide hydrochloride. M/e− 324 for C17H15ClN5 (M+H)+; 1H-NMR (400 MHz, CD3OD) δ 8.27 (d, J=6.6 Hz, 1H), 7.76 (d, J=8.4 Hz, 2H), 7.58 (d, J=9.1 Hz, 1H), 7.46 (d, J=8.4 Hz, 2H), 7.35 (t, J=6.9 Hz, 1H), 6.95 (t, J=6.2 Hz, 1H), 4.46 (s, 2H), 2.37 (s, 3H) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497278B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-0b324460fd564af78edf5e8fb9d394b0 |
| Source note | uspto-grants-2013_07 |