Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propargylamine → 10-Bromo-5,6-dihydro-benzo[f]quinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propargylamine | HCID 239041 | — |
| 반응물 | 8-Bromo-1,2,3,4-tetrahydronaphthalen-2-one | HCID 4136187 | — |
| 생성물 | 10-Bromo-5,6-dihydro-benzo[f]quinoline | HCID 58294583 | 49% |
반응 단계
The title compound is prepared from 8-bromo-2-tetralone and propargylamine following a procedure analogous to that described in Step 1 of Intermediates 1 and 2. Yield: 49% of theory; LC (method 1): tR=2.68 min; Mass spectrum (ESI+): m/z=260/262 (Br) [M+H]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08497281B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-2aa5f87f941543209ef2a59218e28af3 |
| 출처 메모 | uspto-grants-2013_07 |