huagongshe.com
HRID455396

反应详情

EQUATION

反应方程式

HRID 455396 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)c1ccc2nccn2c1
HCID7075376

Imidazo[1,2-a]pyridine-6-carboxylic acid

C8H6N2O2

结构：CN(C)C(On1nnc2cccnc21)=[N+](C)C.F[P-](F)(F)(F)(F)F
HCID9886157

Methanaminium, N-((dimethylamino)(3H-1,2,3-triazolo(4,5-b)pyridin-3-yloxy)methylene)-N-methyl-, hexafluorophosphate(1-) (1:1)

C10H15F6N6OP

结构：c1ccc2c(c1)CC[C@@H]1NCCC[C@H]21
HCID12327022

(4aS,10bR)-1,2,3,4,4a,5,6,10b-Octahydrobenzo[f]quinoline

C13H17N

PRODUCTS

生成物

1
结构：O=C(c1ccc2nccn2c1)N1CCC[C@@H]2c3ccccc3CC[C@@H]21
HCID86654098

未命名化合物

收率 72%

PROCEDURE

实验过程

The title compound is prepared from imidazo[1,2-a]pyridine-6-carboxylic acid and cis-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline following a procedure analogous to that described in Example 1 [2-(7-aza-1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium hexa-fluorophosphate is used]. Yield: 72% of theory; LC (method 3): tR=1.82 min; Mass spectrum (ESI+): m/z=335 [M+H]+.