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HRID455421

反应详情

EQUATION

反应方程式

HRID 455421 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)c1ccc(Cl)c(O)c1
HCID141872

4-Chloro-3-hydroxybenzoic acid

C7H5ClO3

结构：CN(C)C(On1nnc2cccnc21)=[N+](C)C.F[P-](F)(F)(F)(F)F
HCID9886157

Methanaminium, N-((dimethylamino)(3H-1,2,3-triazolo(4,5-b)pyridin-3-yloxy)methylene)-N-methyl-, hexafluorophosphate(1-) (1:1)

C10H15F6N6OP

结构：c1ccc2c(c1)CC[C@@H]1NCCC[C@H]21
HCID12327022

(4aS,10bR)-1,2,3,4,4a,5,6,10b-Octahydrobenzo[f]quinoline

C13H17N

PRODUCTS

生成物

1
结构：O=C(c1ccc(Cl)c(O)c1)N1CCC[C@@H]2c3ccccc3CC[C@@H]21
HCID86654123

未命名化合物

收率 46%

PROCEDURE

实验过程

The title compound is prepared from 4-chloro-3-hydroxy-benzoic acid and cis-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline following a procedure analogous to that described in Example 1 [2-(7-aza-1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium hexa-fluorophosphate is used]. Yield: 46% of theory; LC (method 4): tR=1.99 min; Mass spectrum (ESI+): m/z=342/344 (Cl) [M+H]+.