HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178513517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 178524094 | HCID 178524094 | — |
| Product | HCID 178513517 | HCID 178513517 | 64% |
Reaction Steps
The title compound is prepared from cis-1-(1H-benzoimidazole-5-carbonyl)-2,3,4,4a,9,9a-hexahydro-1H-indeno[2,1-b]pyridine-6-carboxylic acid and ammonia (0.5 mol/L in 1,4-dioxane) following a procedure analogous to that described in Example 1. Yield: 64% of theory; LC (method 1): tR=1.64 min; Mass spectrum (ESI+): m/z=361 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497281B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-d70f424e76684a43ac53ce319629e123 |
| Source note | uspto-grants-2013_07 |