HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178485263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 178524092 | HCID 178524092 | — |
| Product | HCID 178485263 | HCID 178485263 | 19% |
Reaction Steps
The title compound is prepared from cis-1-(1H-benzoimidazole-5-carbonyl)-2,3,4,4a,9,9a-hexahydro-1H-indeno[2,1-b]pyridine-7-carboxylic acid and methylamine (2 mol/L in tetrahydrofuran) following a procedure analogous to that described in Example 1. Yield: 19% of theory; LC (method 1): tR=1.86 min; Mass spectrum (ESI+): m/z=375 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497281B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-ea8cc62fdcd5448dab9c8934d66da5bc |
| Source note | uspto-grants-2013_07 |