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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 455479Generated: October 29, 2026

Methanaminium, N-((dimethylamino)(3H-1,2,3-triazolo(4,5-b)pyridin-3-yloxy)methylene)-N-methyl-, hexafluorophosphate(1-) (1:1) → HCID 178508195, compound

https://huagongshe.com/reaction/455479

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanaminium, N-((dimethylamino)(3H-1,2,3-triazolo(4,5-b)pyridin-3-yloxy)methylene)-N-methyl-, hexafluorophosphate(1-) (1:1)HCID 9886157—
Reactantcis-2,3,4,4a,9,9a-hexahydro-1H-indeno[2,1-b]pyridineHCID 58123900—
ReactantHCID 178508198HCID 178508198—
ProductHCID 178508195HCID 17850819571%

Reaction Steps

The title compound is prepared from 2-amino-1H-benzoimidazole-5-carboxylic acid and cis-2,3,4,4a,9,9a-hexahydro-1H-indeno[2,1-b]pyridine following a procedure analogous to that described in Example 1 [2-(7-aza-1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium hexafluorophosphate is used]. Yield: 71% of theory; LC (method 4): tR=1.64 min; Mass spectrum (ESI+): m/z=333 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08497281B2
Source datasetuspto-grants-2013_07
ORD IDord-689e50aa2d3347bca48c75a3b0088c29
Source noteuspto-grants-2013_07