Iodoethane → HCID 66892231, compound

Participants

Reaction Steps

To a suspension of [6-hydroxy-2′-((4S,5R)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-ylmethyl)-4′-trifluoromethyl-biphenyl-3-yl]-acetic acid (0.085 g, 0.18 mmol) and cesium carbonate (0.171 g, 0.53 mmol) in MeCN was added iodoethane (0.03 mL, 0.35 mmol), and the reaction was stirred at room temperature. The mixture was partitioned between EtOAc and H2O, and the aqueous layer was separated and extracted with EtOAc. The combined organic layers were dried over MgSO4, filtered, and concentrated to give the title compound.

Provenance & Evidence