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HRID456241

反应详情

EQUATION

反应方程式

HRID 456241 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1cc(C(F)(F)F)ccc1Br
HCID7018047

2-Bromo-5-(trifluoromethyl)benzaldehyde

C8H4BrF3O

结构：COC(=O)Cc1ccc(F)c(B2OC(C)(C)C(C)(C)O2)c1
HCID46739456

Methyl [4-fluoro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acetate

C15H20BFO4

PRODUCTS

生成物

1
结构：COC(=O)Cc1ccc(F)c(-c2ccc(C(F)(F)F)cc2C=O)c1
HCID86633169

未命名化合物

PROCEDURE

实验过程

Prepared according to the procedure described in Example 25, Step 3, using the following starting materials: 2-bromo-5-trifluoromethyl-benzaldehyde and [4-fluoro-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acetic acid methyl ester; the isolated product was further purified by preparative HPLC.

WORKUP

后处理

  1. customPrepared
  2. customthe isolated product was further purified by preparative HPLC