HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenylethanol → N-[4-(2-Phenylethoxy)benzoyl]glycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenylethanol | HCID 6054 | — |
| Reactant | Methylparaben | HCID 7456 | — |
| Reactant | N-[4-(2-Cyclopropylethoxy)benzoyl]glycine | HCID 66812105 | — |
| Product | N-[4-(2-Phenylethoxy)benzoyl]glycine | HCID 66812668 | 74% |
Reaction Steps
The same reactions as in Example 9 (9a) and (9b) were conducted using methyl 4-hydroxybenzoate (2.23 g, 14.7 mmol) and 2-phenylethanol (1.80 mL, 15.1 mmol) to give 3.23 g of the title compound (light yellow powder, yield: 74%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497397B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-ea972d666c794969b4a98839a7adb5b0 |
| Source note | uspto-grants-2013_07 |