Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(4-Hydroxybenzoyl)glycine tert-butyl ester → N-[4-(2-Cyclopenta-2-en-1-ylethoxy)benzoyl]glycine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(4-Hydroxybenzoyl)glycine tert-butyl ester | HCID 10682169 | — |
| 반응물 | 2-Cyclopentene-1-ethanol | HCID 10964444 | — |
| 생성물 | N-[4-(2-Cyclopenta-2-en-1-ylethoxy)benzoyl]glycine | HCID 66812182 | 72% |
반응 단계
The same reaction as in Example 1 (1b) was conducted using N-(4-hydroxybenzoyl)glycine tert-butyl ester (157 mg, 0.625 mmol) prepared in Example 1 (1a) and 2-cyclopenta-2-en-1-ylethanol (which is the compound disclosed in J. Org. Chem., (2000), 65, 4241-4250, 85 mg, 0.75 mmol) to give 128 mg of the title compound (white powder, yield: 72%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08497397B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-177f8dac70334486b69579511e496689 |
| 출처 메모 | uspto-grants-2013_07 |