Sulfuryl chloride → HCID 68554334, compound

Participants

Reaction Steps

The product from Example 23, Part B (100 mg, 0.17 mmol) was dissolved in dichloromethane (1.7 ml). TEA (84 ul, 0.6 mmol) was added followed by the sulfonyl chloride (65.6 mg, 0.34 mmol). The reaction was stirred overnight then loaded onto a silica plug and eluted with ethyl acetate to give the title compound as a white solid (112 mg, 93% yield). MS (APCI) m/z 699 [M+H]+.

Provenance & Evidence