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HRID456387

反应详情

EQUATION

反应方程式

HRID 456387 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)NN
HCID70091

Hydrazinecarboxylic acid, 1,1-dimethylethyl ester

C5H12N2O2

结构：CC(C)(C)OC(=O)N1CCC(=O)CC1
HCID735900

1-Boc-4-piperidone

C10H17NO3

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NN=C1CCN(C(=O)OC(C)(C)C)CC1
HCID20824233

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC
溶剂HCID8058

n-Hexane

C6H14

PROCEDURE

实验过程

A mixture of 0.15 mole of 4-oxo-piperidine-1-carboxylic acid tert-butyl ester (commercially available) and 0.15 mole of tert-butylcarbazate in 250 ml of hexane is stirred for 18 h at RT. The precipitate is filtered off and dried under vacuum. M. p. 172–174° C.

WORKUP

后处理

  1. filtrationThe precipitate is filtered off
  2. customdried under vacuum