HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 135517309, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Benzoyl chloride, 3-chloro- | HCID 69252 | — |
| Reactant | HCID 136358049 | HCID 136358049 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 135517309 | HCID 135517309 | 32% |
Reaction Steps
2,2-Dimethyl-propionic acid 5-amino-3-(1H-pyrrol-2-yl)-indazol-1-yl ester (0.38 mmol) (From Example 28) was coupled with 3-chloro-benzoyl chloride (0.4 mmol) and triethylamine in DCM at 0° C. to give 41 mg of the titled compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07186716B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-4536509632d2464f8f12dd3255230fcc |
| Source note | uspto-grants-2007_03 |